Details
Factory Supply Industrial Grade Methyl 3-iodobenzoate 618-91-7 with Best Price
- Molecular Formula: C8H7IO2
- Molecular Weight: 262.047
- Appearance/Colour: Pale yellow crystals
- Vapor Pressure: 0.00298mmHg at 25°C
- Melting Point: 54-57 °C
- Refractive Index: 1.597
- Boiling Point: 284.4 °C at 760 mmHg
- Flash Point: 125.8 °C
- PSA： 26.30000
- Density: 1.753 g/cm3
- LogP: 2.07780
Methyl 3-iodobenzoate(Cas 618-91-7) Usage
InChI:InChI=1/C8H7IO2/c1-11-8(10)6-3-2-4-7(9)5-6/h2-5H,1H3
618-91-7 Relevant articles
-
Kondo,Ikeda
, (1940)
-
Cyclometalated iridium complex as well as preparation method and application thereof
-
Paragraph 0043-0046, (2021/05/01)
The invention belongs to the technical f...
Hydrogen-Bond-Donor Solvents Enable Catalyst-Free (Radio)-Halogenation and Deuteration of Organoborons
Yang, Yi,Gao, Xinyan,Zeng, Xiaojun,Han, Junbin,Xu, Bo
supporting information, p. 1297 - 1300 (2020/12/23)
A hydrogen bond donor solvent assisted (...
Bimetallic Cooperative Catalysis for Decarbonylative Heteroarylation of Carboxylic Acids via C-O/C-H Coupling
Liu, Chengwei,Ji, Chong-Lei,Zhou, Tongliang,Hong, Xin,Szostak, Michal
supporting information, p. 10690 - 10699 (2021/04/09)
Cooperative bimetallic catalysis is a fu...
Design, synthesis, and biological evaluations of novel 3-amino-4-ethynyl indazole derivatives as Bcr-Abl kinase inhibitors with potent cellular antileukemic activity
El-Damasy, Ashraf K.,Jin, Heewon,Seo, Seon Hee,Bang, Eun-Kyoung,Keum, Gyochang
, (2020/09/22)
Breakpoint cluster region-Abelson (Bcr-A...
618-91-7 Process route
-
-
67-56-1
methanol
-
-
618-51-9
3-Iodobenzoic acid
-
-
618-91-7
methyl 3-iodo-benzoate
| Conditions | Yield |
|---|---|
|
With
sulfuric acid;
for 2.5h;
Schlenk technique;
Inert atmosphere;
|
99%
|
|
With
sulfuric acid;
for 2.5h;
Reflux;
Inert atmosphere;
|
99%
|
|
With
sulfuric acid;
for 2.5h;
Inert atmosphere;
Reflux;
|
97%
|
|
With
sulfuric acid;
at 80 ℃;
for 24h;
|
97%
|
|
sulfuric acid;
for 24h;
Reflux;
|
96.5%
|
|
With
sulfuric acid;
for 30h;
Reflux;
|
96%
|
|
With
sulfuric acid;
for 21h;
Reflux;
|
96%
|
|
With
sulfuric acid;
for 48h;
Reflux;
|
95%
|
|
With
sulfuric acid;
for 24h;
Reflux;
|
94.65%
|
|
With
thionyl chloride;
at 0 - 20 ℃;
for 16h;
|
93%
|
|
With
sulfuric acid;
at 70 ℃;
for 5h;
|
81%
|
|
With
Oxone;
In
toluene;
at 60 ℃;
for 48h;
Green chemistry;
|
81%
|
|
With
sulfuric acid;
Heating;
|
80%
|
|
With
thionyl chloride; N,N-dimethyl-formamide;
at 80 ℃;
for 18h;
|
78.4%
|
|
With
sulfuric acid;
for 3h;
Reflux;
|
57%
|
|
With
hydrogenchloride;
|
|
|
With
sulfuric acid;
|
|
|
With
hydrogenchloride;
In
diethyl ether;
at 20 ℃;
for 24h;
|
|
|
With
sulfuric acid;
at 60 ℃;
Inert atmosphere;
|
|
|
With
thionyl chloride;
at 40 ℃;
for 1h;
|
|
|
With
sulfuric acid;
at 80 ℃;
for 6h;
|
-
-
1877-71-0
benzene 1,3-dicarboxylic acid monomethyl ester
-
-
618-91-7
methyl 3-iodo-benzoate
| Conditions | Yield |
|---|---|
|
With
N-iodo-succinimide; [4,4′-bis(1,1-dimethylethyl)-2,2′-bipyridine-N1,N1′]bis{3,5-difluoro-2-[5-(trifluoromethyl)-2-pyridinyl-κN]phenyl-κC}iridium(III) hexafluorophosphate; iodine; caesium carbonate;
In
1,2-dichloro-ethane;
at 50 ℃;
for 24h;
Inert atmosphere;
Irradiation;
Sealed tube;
|
75%
|
618-91-7 Upstream products
-
4518-10-9
Methyl 3-aminobenzoate
-
67-56-1
methanol
-
618-51-9
3-Iodobenzoic acid
-
186581-53-3
diazomethane
618-91-7 Downstream products
-
7775-64-6
3-(1-naphthyl)benzoic acid
-
39115-94-1
3-iodobenzhydrazide
-
1751-97-9
biphenyl-3,3'-dicarboxylic acid dimethyl ester
-
854237-02-8
methyl 3-(1-formyl-3,4-methylenedioxy)benzoate
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